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type="text/css"></style> <div id="ct" class="ct2 wp cl"> <div class="mn"> <div class="bm_haa cl"> <div class="bm_h cl"> <a href="http://www.oecr.com/portal.php?mod=rss&catid=58" class="y xi2 rss" target="_blank" title="RSS">订阅</a><h1 class="xs2">文章</h1> </div></div> <div class="kjkjb"> <div class="bm vw" style="margin-bottom:0;"> <div class="h hm"> <div class="zxtoux"><img src="http://www.oecr.com/uc_server/avatar.php?uid=54876&size=small" /></div> <h1 class="ph">纳米反应器研究取得新成果 </h1> <p class="xg1"> 时间：2012-9-13 17:16<a class="zz" href="home.php?mod=space&uid=54876">作者：update</a> 阅读<em id="_viewnum">(2555)</em> 评论: 0</p> <div class="zxfb" ><a href="http://www.oecr.com/portal.php?mod=rss&catid=58" class="y xi2 rss" target="_blank" title="RSS">订阅</a></div> </div> <!--[diy=diysummarytop]--><div id="diysummarytop" class="area"></div><!--[/diy]--> <div class="s"> <div class="ss"><div><span>导读： </span>中科院大连化学物理研究所杨启华研究员领导的科研团队在纳米反应器的制备与应用方面取得新成果。相关结果以研究通讯的形式发表在德国《应用化学》杂志上(Angew. Chem. Int. Ed., 2012, 51(36), 9164–9168.)，并被选 ...</div> </div> <!--[diy=diysummarybottom]--><div id="diysummarybottom" class="area"></div><!--[/diy]--> <div class="d"> <!--[diy=diycontenttop]--><div id="diycontenttop" class="area"></div><!--[/diy]--> <table cellpadding="0" cellspacing="0" class="vwtb"><tr><td id="article_content">中科院大连化学<a href="http://theory.oecr.com" target="_blank" class="relatedlink">物理</a>研究所杨启华研究员领导的科研团队在<a href="http://material.oecr.com" target="_blank" class="relatedlink">纳米</a>反应器的制备与应用方面取得新成果。相关结果以研究通讯的形式发表在德国《应用化学》杂志上(Angew. Chem. Int. Ed., 2012, 51(36), 9164–9168.)，并被选为当期的“热点论文”。<br> <br>在自然界中，化学转化往往以串联反应的形式在限域的空间内完成，这种限域的空间可以是几个纳米的酶也可以是微米级的细胞。受自然界的启发，化学家尝试构建各种微/纳米反应器，以期能够实现高效和连续的化学转化。杨启华研究员领导的研究组多年来在微/纳米反应器的合成和催化应用方面开展研究工作，发展了有机硅源辅助溶解无机氧化硅的制备“蛋黄-蛋壳型”纳米反应器的新方法(Chem. Mater., 2011, 23, 3676)，向核-壳氧化硅的合成体系中添加有机硅源，可以在构建有机氧化硅外壳的同时诱发无机氧化硅的溶解，从而形成“蛋黄-蛋壳型”纳米<a href="http://material.oecr.com" target="_blank" class="relatedlink">材料</a>。<br> <br>最近，该研究组基于前期的研究进展，通过引入氧化硅牺牲层，实现了不同无机氧化硅层的选择性溶解，得到具有蛋黄-蛋壳型结构的纳米材料。与其它制备方法相比，该方法可以在核或壳的形成过程中可控引入不同的功能基团，从而选择性地对材料的核或壳进行功能化。基于以上方法，该研究组成功制备了具有碱性核和酸性壳的“蛋黄-蛋壳型”纳米反应器，并且通过表征证实了酸、碱基团是分别分布在材料的壳和核上。该纳米反应器在Deacetalization–Henry串联反应中表现出高活性、高选择性和稳定性。很多具有后修饰潜能的功能基团（-NH2, -SH等）和纳米粒子（Pd, Pt等）可以被精确的引入到材料的核或壳中。<br> <br>可以预见，该方法可实现不同种类活性组分（比如聚合物、酶等）的精确定位，为制备多功能的纳米反应器提供了一个有效途径。Materials Views China杂志以“具有碱性核和酸性壳的纳米反应器”为题，对该研究工作作了专门评述，高度评价了该研究工作的意义。该研究得到了国家自然科学基金和973项目的资助。 <DIV><FONT color="#808080" size=2><IMG src="http://www.oecr.com/xwb/images/bgimg/icon_logo.png"> 已同步至 <a href="http://api.t.sina.com.cn/2200118572/statuses/3489851955523309" target="_blank">update的微博</A></FONT></DIV></td></tr></table> <!--[diy=diycontentbottom]--><div id="diycontentbottom" class="area"></div><!--[/diy]--> <script src="data/cache/home.js?eOg" 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